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Instrument Description

The AFCI glovebox, located inside of the Fuel Manufacturing Facility, is used for transuranic fuel fabrication activities. The glovebox windows and gloves are shielded to provide radiological dose reduction. It is maintained under an atmosphere of purified argon, helium, or a mixture of argon or helium, to levels of <10 ppm oxygen. Glovebox equipment includes standard powder processing equipment, such as a high-energy ball mill, press, and high-temperature tantalum element vacuum furnace. In addition to powder processing equipment, there are horizontal and vertical tube furnaces, which can be used in a vacuum, hydrogen, argon, or wet argon environment and a Centorr Series 5SA arc melter. Co-located with the AFCI glovebox is an X-ray radiography system. The system is composed of a 160 KeV X-ray tube, and images can be captured and processed digitally.



The AFCI glovebox is used to fabricate metallic and ceramic fuel forms, as well as to provide an inert environment for sample preparation and fuel irradiation test assembly. Samples can be fabricated, encapsulated in cladding tubes, and removed from the glovebox line with no external contamination.

The Centorr 5SA arc melting is ideal for transuranic alloy production on the scale of 10-50 grams, and casting simple shapes that can be incorporated into fuel irradiation test. A vertical tube furnace is currently configured to americium purification through distillation but can be configured for a number of different applications. The powder processing equipment, including the high-temperature vacuum furnace, can be used for ceramic fuel fabrication or similar powder metallurgy processes. A horizontal standard tube furnace can also be used for powder processing.

The radiography system is routinely used for weld radiography as part of fuel irradiation test assembly. However, it can also be used to radiograph any number of clad radiological items, for example, small shipping containers, storage cans, etc.   

Instrument sample preparation area; Shielded optical microscopy vacuum testing chambers testing properties gross and isotopic gamma scanning; Instron remote load frame gas measurement and analysis accident condition simulator furnace extrusion; Metallic fuel line; Advanced Fuel Cycle Initiative glovebox; Glovebox advance casting system furnace; Metallic fuel line; Metallic fuel line handling; Inert-radiological gloveboxes; Uranium handling repackaging glovebox; Transuranic breakout glovebox gamma irradiator surveillance glovebox line; Cell area Quanta 3D FEG dual-beam SEM FIB JSM-7000f SEM; Gatan precision etching and coating system; Gatan precision ion polishing systems II; Gatan precision ion polishing systems JEM 2010 STEM Cameca SX100R EPMA FEI QUANTA 3D FEG Titan ChemiSTEM FEG-STEM FEI Helios dual-beam SEM-plasma FIB diffraction; Micro X-ray diffractometer Di LemmaJEOL JSM-7000f SEM coupled plasma-mass spectrometer coupled plasma-atomic emission spectrometer; Thermal Ionization Mass Spectrometer coupled plasma-mass spectrometer advance casting system furnace; Hot uniaxial press furnace mass spectrometer; ELTRA CS-800; ELTRA ONH-2000 furnace; Differential scanning calorimeter; Simultaneous thermal analyzer; Pushrod dilatometer; Laser flash analyzer Separator Laboratories X-ray diffractometer; X-ray diffraction; Hot uniaxial press furnace
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