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Skip Navigation LinksJEOL JEM 2010 STEM

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Instrument Description


The JEOL JEM-2010 TEM/STEM at EML is a 200KV transmission electron microscope. It has an analytical resolution pole piece in high-contrast configuration. The TEM image is recorded on a Gatan UltraScan 1000 digital camera with 2048x2048 pixels in 16 bits over a roughly 0.8x0.8-inch image area on the large phosphorous screen. The STEM probe size is 15, 20, and 25 nm. The Bruker SDD EDS detector allows fast EDS analysis including elemental line scanning and 2-D mapping. The retractable SDD detector allows for TEM analysis of a highly radioactive sample without composition analysis. In addition to the standard double-tilt analytical holder, the TEM is equipped with a double-tilt heating holder (Gatan model: 652.MA) with maximum temperature up to 850°C.


Applications


  • Microstructural defects analysis for irradiated fuel and materials.

  • Thermal stability and phase stability studies with TEM in-situ heating experiment.

  • High-resolution chemical analysis (25 nm) with SDD in STEM mode.


Specifications


  • Magnification: 1,000x to 800,000x

  • Resolution: 0.23 nm at 200 kV

  • Acceleration voltage: 80 to 200 kV


  
  
  
Instrument
  
  
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https://bios.inl.gov/BioPhotos/CraigDees.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Craig%20DeesVibration testing
  
https://bios.inl.gov/BioPhotos/KevinGeddes.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Kevin%20GeddesMass properties
  
https://bios.inl.gov/BioPhotos/KatelynWheeler.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Katelyn%20WheelerPrecision gross and isotopic gamma scanning; Instron remote load frame
  
https://bios.inl.gov/BioPhotos/DavidSell.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=David%20SellFission gas measurement and analysis
  
https://bios.inl.gov/BioPhotos/CadChristensen.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Cad%20ChristensenFuel accident condition simulator furnace
  
https://bios.inl.gov/BioPhotos/RandallFielding.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Randall%20FieldingUranium extrusion; Metallic fuel line; Advanced Fuel Cycle Initiative glovebox; Glovebox advance casting system furnace; Metallic fuel line; Metallic fuel line
  
https://bios.inl.gov/BioPhotos/CurtisClark.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Curtis%20ClarkUranium handling; Inert-radiological gloveboxes; Uranium handling
  
https://bios.inl.gov/BioPhotos/CoryBrower.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Cory%20BrowerNeptunium repackaging glovebox; Transuranic breakout glovebox
  
https://bios.inl.gov/BioPhotos/DeanPeterman.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Dean%20PetermanCobalt-60 gamma irradiator
  
https://bios.inl.gov/BioPhotos/larryevens.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Larry%20EvensTransuranic surveillance glovebox line; Cell area
  
https://bios.inl.gov/BioPhotos/danieljadernas.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Daniel%20JadernasFEI Quanta 3D FEG dual-beam SEM FIB
  
https://bios.inl.gov/BioPhotos/Jan-FongJue.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Jan-Fong%20JueJEOL JSM-7000f SEM; Gatan precision etching and coating system; Gatan precision ion polishing systems II; Gatan precision ion polishing systems
  
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https://bios.inl.gov/BioPhotos/KarenWright.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Karen%20WrightShielded Cameca SX100R EPMA
  
https://bios.inl.gov/BioPhotos/Danielmurray.JPGhttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Daniel%20MurrayShielded FEI QUANTA 3D FEG
  
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https://bios.inl.gov/BioPhotos/CortneyPincock.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Cortney%20PincockInductively coupled plasma-mass spectrometer
  
https://bios.inl.gov/BioPhotos/MatthewJones.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Matthew%20JonesInductively coupled plasma-atomic emission spectrometer; Thermal Ionization Mass Spectrometer
  
https://bios.inl.gov/BioPhotos/MagenColeman.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Magen%20ColemanMulti-collector-inductively coupled plasma-mass spectrometer
  
https://bios.inl.gov/BioPhotos/ScottWilde.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Scott%20WildeGlovebox advance casting system furnace; Hot uniaxial press furnace
  
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https://bios.inl.gov/BioPhotos/CynthiaAdkins.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Cynthia%20AdkinsTube furnace; Differential scanning calorimeter; Simultaneous thermal analyzer; Pushrod dilatometer; Laser flash analyzer
  
https://bios.inl.gov/BioPhotos/JaredHorkley.jpghttps://mfctemp.inl.gov/SitePages/Biography.aspx?Title=Jared%20HorkleyMass Separator Laboratories
  
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